Biosynthesis, Characterisation, and Antioxidant Activity of Silver Nanoparticles using Schinus molle L.      
Yazarlar (7)
Prof. Dr. Ramazan ERENLER Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Radıa Chaouıa
Université Blida 1, Cezayir
Doç. Dr. İlyas YILDIZ Iğdır Üniversitesi, Türkiye
Doç. Dr. Nusret GENÇ Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Doç. Dr. Esma Nur GEÇER Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Cengiz Temiz
Zonguldak Bülent Ecevit Üniversitesi, Türkiye
Salah Akkal
Université Constantine 1, Cezayir
Makale Türü Açık Erişim Özgün Makale
Makale Alt Türü SCOPUS dergilerinde yayınlanan tam makale
Dergi Adı Trends in Sciences
Dergi ISSN 2774-0226 Scopus Dergi
Dergi Tarandığı Indeksler Scopus
Makale Dili İngilizce
Basım Tarihi 06-2023
Cilt No 20
Sayı 10
DOI Numarası 10.48048/tis.2023.6105
Makale Linki http://dx.doi.org/10.48048/tis.2023.6105
Özet
Schinus molle L. has been used as a folk medicine for many years. The aim of this study is to synthesize the silver nanoparticles, to identify them by spectroscopic techniques and to evaluate the antioxidant effects. In this study, Schinus molle was extracted with hexane, dichloromethane, ethyl acetate and methanol successively. After removal of the solvent from each extract by reduced pressure, the crude extracts were yielded. Methanol extract was used for synthesis of silver nanoparticles (s-AgNPs). The methanol extract dissolved in distilled water was treated with silver nitrate solution to produce the s-AgNPs. The extensive spectroscopic study enabled the identification of synthesized s-AgNPs. UV-Vis spectroscopic analysis presented the maximum absorption of s-AgNPs at 486 nm. The average particle size of s-AgNPs was measured as 77.6 nm by Scanning electron microscope (SEM). X-ray diffraction (XRD) pattern revealed that the nanoparticles were face-centered cubic structure. The slight differences between extract and AgNPs in FTIR spectrum proved the formation of s-AgNPs. In that, some functional group such as hydroxyl in the extract was oxidized while reduction of silver ions. Elemental analysis displayed the silver percentage to be 75.79 %w/w. Antioxidant activity study including DPPH, ABTS•+ and FRAP assays displayed the considerable effect of s-AgNPs. This is the first report to present the synthesis of silver nanoparticles from Schinus molle L. methanol extract and to evaluate the antioxidant activity.
Anahtar Kelimeler
Antioxidant activity | Nanoparticles | Schinus molle | Spectroscopy