Fabrication of cobalt nano particles by pulsed wire evaporation method in nitrogen atmosphere     
Yazarlar (7)
Prof. Dr. Fikret YILMAZ Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Dong Jın Lee
Nano Technology Inc., Güney Kore
Joon Woo Song
Kongju National University, Güney Kore
Hyun Seon Hong
Institue For Advanced Engineering, Korea, Güney Kore
Hyeon Taek Son
Korea Institute Of Industrial Technology, Güney Kore
Jae Sık Yoon
Korea Basic Science Institute, Güney Kore
Soon Jık Hong
Kongju National University, Güney Kore
Makale Türü Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale
Dergi Adı Powder Technology
Dergi ISSN 0032-5910 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Dergi Grubu Q4
Makale Dili İngilizce
Basım Tarihi 02-2013
Cilt No 235
Sayı 1
Sayfalar 1047 / 1052
DOI Numarası 10.1016/j.powtec.2012.10.024
Makale Linki http://linkinghub.elsevier.com/retrieve/pii/S0032591012007012
Özet
This work reports the use of pulsed wire evaporation (PWE) method to prepare cobalt (Co) nano-particles. The effect of charging voltage on the average particle size and particle morphology was studied. The Co nano-particles were characterized by means of scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and BET surface area analysis. SEM and TEM observations showed that the Co particles had spherical shape and were linked to each other because of their magnetic property. The XRD analyses confirmed that Co nano-particles had FCC structure without any presence of impurity phase. Average particle size was calculated by three methods; TEM, BET and XRD. The results showed that the particle size decreased with increasing charging voltage and then attempted to saturate, which was explained with crystallite size of the Co wire, superheating factor and specific energy input into the wire. © 2012 Elsevier B.V.
Anahtar Kelimeler
Charging voltage | Nanofabrication | Nanostructured materials | Particle size | Pulsed wire evaporation