Biosynthesis, characterization and antioxidant activity of oleuropein-mediated silver nanoparticles       
Yazarlar (6)
Doç. Dr. Nusret GENÇ Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Doç. Dr. İlyas YILDIZ Iğdır Üniversitesi, Türkiye
Radıa Chaou
Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Prof. Dr. Ramazan ERENLER Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Cengiz Temiz
Zonguldak Bülent Ecevit Üniversitesi, Türkiye
Mahfuz Elmastaş
University Of Health Sciences, Türkiye
Makale Türü Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale
Dergi Adı Inorganic and Nano Metal Chemistry
Dergi ISSN 2470-1556 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Dergi Grubu Q3
Makale Dili İngilizce
Basım Tarihi 07-2020
Cilt No 51
Sayı 1
Sayfalar 1 / 9
DOI Numarası 10.1080/24701556.2020.1792495
Makale Linki http://dx.d24701556.2020.1792495oi.org/10.1080/
Özet
In this study, oleuropein was isolated from olive leaves by chromatographic method and its structure was elucidated by spectroscopic analyses such as FTIR, 1H-NMR and 13CNMR. Silver nanoparticles (AgNPs) were synthesized using oleuropein and their antioxidant activity was investigated using DPPH, ABTS•+, and FRAP assays. The AgNPs were characterized by UV-Vis, FT-IR, XRD, and SEM analyses. The absorption peak at 450 nm in UV-Vis spectrum confirmed the AgNPs formation. Scanning electron microscope (SEM) identified the formation of spherical-shaped nanoparticles with the average size of 71 nm. Rietveld analysis was carried out by X-ray diffraction data with High Score Plus software. XRD with 2θ degrees at 38.1°, 44.3°, 64.4° and 77.4° can be assigned to the (111), (200), (220) and (311) Bragg’s reflections of the face-centered cubic crystalline structure. Biosynthetic nanoparticles revealed more inhibitory effect (5.22, IC50, µg/mL) against ABTS•+ than standard BHT (7.03, IC50, µg/mL).
Anahtar Kelimeler
antioxidant activity | Nanoparticles | natural product | oleuropein