Bromination of 5-Methoxyindane: Synthesis of New Benzoindenone Derivatives and Ready Access to 7H-Benzo[c]fluoren-7-one Skeleton
Yazarlar (4)
Ahmet Tutar Sakarya Üniversitesi, Türkiye
Doç. Dr. Kıymet BERKİL AKAR Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Richard R Hark
| Makale Türü |
Özgün Makale
(SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
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| Dergi Adı | SYNTHETIC COMMUNICATIONS (Q4) | ||
| Dergi ISSN | 0039-7911 Wos Dergi Scopus Dergi | ||
| Dergi Tarandığı Indeksler | SCI-Expanded | ||
| Makale Dili | İngilizce | Basım Tarihi | 01-2008 |
| Cilt / Sayı / Sayfa | 38 / 9 / 1333–1345 | DOI | 10.1080/00397910801916223 |
| Makale Linki | http://dx.doi.org/10.1080/00397910801916223 | ||
| Özet |
| The photobromination of 5‐methoxyindane and 5‐methoxyindanone was studied at both high and low temperatures. 1,2,3‐Tribromo‐6‐methoxyindene was easily synthesized by photolytic bromination of 5‐methoxyindane at low temperature. 1,1,2,3‐Tetrabromo‐6‐methoxyindene was obtained from the photobromination of 5‐methoxyindan at 77 °C, which could then be easily converted to the 2,3‐dibromo‐6‐methoxyindene by silver‐supported hydrolysis. Photochemical bromination of 5‐methoxy‐1‐indanone with N‐bromosuccinimide (NBS) gave 3‐bromo‐6‐methoxyindene, which upon thermolysis gave a benzo[c]fluorenone derivative. |
| Anahtar Kelimeler |
| benzo[c] fluorenone | indenone | photobromination |
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| Google Scholar | 23 |
| Web of Science | 14 |