Synthesis and Characterization of a Novel Conformation of 2,9,10-Tribromoanthracene-1,4-dione
Yazarlar (3)
Doç. Dr. Kıymet BERKİL AKAR Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Osman Çakmak İstanbul Rumeli Üniversitesi, Türkiye
Ertan Şahin Atatürk Üniversitesi, Türkiye
| Makale Türü |
Özgün Makale
(SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
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| Dergi Adı | JOURNAL OF CHEMICAL CRYSTALLOGRAPHY (Q4) | ||
| Dergi ISSN | 1074-1542 Wos Dergi Scopus Dergi | ||
| Dergi Tarandığı Indeksler | SCI-Expanded | ||
| Makale Dili | İngilizce | Basım Tarihi | 12-2013 |
| Cilt / Sayı / Sayfa | 43 / 12 / 677–684 | DOI | 10.1007/s10870-013-0472-4 |
| Makale Linki | http://dx.doi.org/10.1007/s10870-013-0472-4 | ||
| Özet |
| Synthesis and X-ray analysis of single crystals of 2,9,10-tribromoanthracene-1,4-dione 4 has been described and its novel conformation is reported. Single crystals were grown by slow evaporation technique from toluene solution at −15 °C. The compounds have been characterized by elemental analysis, FT-IR, Mass and NMR spectroscopy. The compound crystallizes in the triclinic space group P−1 with unit cell dimensions a = 7.6842(2), b = 9.4865(2), c = 19.9388(4) Å, α = 78.784(5), β = 76.980(5), γ = 67.834(4) Å; V: 1,301.75(7) Å3; Z = 2, R1 = 0.0748, and wR2 = 0.131.Graphical Abstract |
| Anahtar Kelimeler |
| 1,4-Anthraquinone | Bromoanthraquinone | Single crystals | X-ray diffraction |
BM Sürdürülebilir Kalkınma Amaçları
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| Google Scholar | 3 |
| Web of Science | 3 |