Determination of Chloroanisoles and Chlorophenols In Cork and Wine by using HS-SPME and GC-ECD Detection     
Yazarlar (4)
Rahmi Ertan Anlı
Ankara Üniversitesi, Türkiye
Didehan Özhan
Vural Nilüfer
Prof. Dr. Mustafa BAYRAM Ankara Üniversitesi, Türkiye
Makale Türü Açık Erişim Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale
Dergi Adı Journal of the Institute of Brewing
Dergi ISSN 2050-0416 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI
Dergi Grubu Q3
Makale Dili İngilizce
Basım Tarihi 01-2009
Cilt No 115
Sayı 1
Sayfalar 71 / 77
DOI Numarası 10.1002/j.2050-0416.2009.tb00346.x
Özet
Cork taint is an off‐flavor problem in wine, the main reason being the presence of 2,4,6‐trichloroanisole (TCA) in the cork stopper. In addition to the TCA, the presence of other chloroanisole and chlorophenol family compounds (the perception limits of which are very low) can also result in, or contribute to, cork taint problem. In this study, the levels of 2,4‐dichloroanisole (DCA), 2,4,6‐trichloroanisole (TCA), 2,3,4,6‐tetrachloroanisole (TeCA), pentachloroanisole (PCA), 2,4,6‐trichlorophenol (TCP), 2,3,4,6‐tetrachlorophenol (TeCP) and penthaclorophenol (PCP) were assayed in cork stoppers (natural, agglomerated and colmate) and in red wine samples from different wineries in Turkey using HS‐SPME and GC‐ECD detection. The performance parameters for all chloroanisole and chlorophenol compounds were as follows: recovery 92.48–102.53%, R 0.992‐0.996. The LOQ values were DCA (8.4 ng/L), TCA (0.8 ng/L …
Anahtar Kelimeler
chloroanisoles | chlorophenols | cork | cork taint | HS-SPME (HeadSpace-Solid Phase Microextraction) | GC-ECD (Gas Chromatography-Electron Capture Detection) | wine