Synthesis and electroanalytical applications of a novel hydrazinecarbothioamide derivative molecule
Yazarlar (5)
Doç. Dr. Oğuz ÖZBEK Zonguldak Bülent Ecevit Üniversitesi, Türkiye
Öğr. Gör. Serkan Ören Zonguldak Bulent Ecevit University, Türkiye
Prof. Dr. Meliha Burcu GÜRDERE Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Prof. Dr. Ömer IŞILDAK Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Prof. Dr. Mustafa CEYLAN Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Makale Türü Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı Chemical Papers (Q3)
Dergi ISSN 0366-6352 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Makale Dili Türkçe Basım Tarihi 07-2023
Cilt / Sayı / Sayfa 77 / 11 / 6679–6687 DOI 10.1007/s11696-023-02968-0
Makale Linki http://dx.doi.org/10.1007/s11696-023-02968-0
UAK Araştırma Alanları
Analitik Kimya Elektrokimya Spektroskopi
Özet
Molecules containing multiple donor atoms such as nitrogen, oxygen and sulfur in their structure are more preferred as ionophores in the preparation of ion-selective electrodes. In this study, a new hydrazinecarbotioamide derivative molecule was synthesized as an ionophore and characterized using NMR, FT–IR and elemental analysis techniques. The potentiometric electrodes prepared with the synthesized new molecule (ionophore) exhibited selectivity towards lead(II) ions. This novel electrode had a low detection limit of 6.98 × 10–7 M over a wide concentration range of 1.0 × 10–6–1.0 × 10–1 M. Obtained experimental data showed that the electrode has good repeatability, good selectivity and good stability. At the same time, it could work in a wide pH range without being affected by pH changes. The analytical applications of the developed electrode, whose potentiometric performance parameters were …
Anahtar Kelimeler
Hydrazinecarbothioamide | Ionophore | Lead(II) | Potentiometry | Synthesis
BM Sürdürülebilir Kalkınma Amaçları
Atıf Sayıları
Scopus 6
Google Scholar 6
Synthesis and electroanalytical applications of a novel hydrazinecarbothioamide derivative molecule

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