NiO nanoparticles via calcination of a Schiff base complex: Photocatalytic and microbicidal activity     
Yazarlar (2)
Doç. Dr. Ayşegül ŞENOCAK Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Rizvan İmamoğlu
Bartin Üniversitesi, Türkiye
Makale Türü Açık Erişim Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale
Dergi Adı Indian Journal of Chemical Technology
Dergi ISSN 0971-457X Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Dergi Grubu Q4
Makale Dili İngilizce
Basım Tarihi 09-2022
Cilt No 29
Sayı 5
Sayfalar 540 / 546
DOI Numarası 10.56042/ijct.v29i5.62576
Makale Linki http://nopr.niscpr.res.in/handle/123456789/60427
Özet
Calcination method has been used to create NiO nanoparticles with a diameter of 19 to 30 nm from [NiL] [L: 2,2'-((1E,1'E)-(1,2-phenylenebis(azanylylidene))bis(methanylylidene))bis(4-bromophenolate)]. Formation and purity of the NiO nanoparticles produced under mild conditions without any special needs are evidenced by fourier-transformed infrared (FT-IR) spectroscopy, ultraviolet visible (UV-Vis) spectroscopy, X-ray powder diffraction (XRD), energy-dispersive X-ray (EDX) spectroscopy and scanning transmission electron microscopy (STEM). According to the spectral methods, transformation of the synthesized nickel-Schiff base complex into the nanoparticles has been achieved with high purity, high crystallinity and low agglomeration by thermal decomposition which is an efficient and simple approach. The nanoparticles are employed as a catalyst for the decomposition of methylene blue, an industrial synthetic dye, and the nanoparticles exhibit mild photocatalytic activity. Furthermore, biological activity of nanoparticles has been investigated on five bacterial strains and two fungi, with promising results.
Anahtar Kelimeler
Biological Activity | Calcination | Catalytic Activity | Industrial dyes | NiO nanoparticles