Ultrasonication ionic liquid based dispersive liquid liquid microextraction of palladium in water samples and determination of microsampler system assisted FAAS
Yazarlar (2)
Prof. Dr. Demirhan ÇITAK
Tokat Gaziosmanpaşa Üniversitesi, Türkiye
Prof. Dr. Mustafa TÜZEN
Tokat Gaziosmanpaşa Üniversitesi, Türkiye
| Makale Türü |
Özgün Makale
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| Makale Alt Türü | SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale |
| Dergi Adı | Desalination and Water Treatment |
| Dergi ISSN | 1944-3994 Wos Dergi Scopus Dergi |
| Dergi Tarandığı Indeksler | SCI-Expanded |
| Dergi Grubu | Q4 |
| Makale Dili | İngilizce |
| Basım Tarihi | 03-2015 |
| Cilt No | 53 |
| Sayı | 10 |
| Sayfalar | 2686 / 2691 |
| DOI Numarası | 10.1080/19443994.2013.868838 |
| Makale Linki | http://www.tandfonline.com/doi/abs/10.1080/19443994.2013.868838 |
| Özet |
| In the proposed approach, a simple and efficient ultrasonication ionic liquid-based dispersive liquid–liquid microextraction (UIL-DLLME) was described. Microsampler system-assisted flame atomic absorption spectrometer was used at the determination step of Pd(II). 1-Phenylthiosemicarbazide (PTC) and 1-hexyl-3-methyl imidazolium bis(trifluoromethylsulfonyl)imide [C6mim][Tf2N] were used as the chelating agent and the extraction solvent of UIL-DLLME, respectively. Ultrasonication was used for dispersing of [C6mim][TF2N] into samples. Different experimental conditions affecting UIL-DLLME of Pd(II) were examined and optimized. The analytical performance characteristics of investigated method including limit of quantification (33 μg L−1), limit of detection (11 μg L−1), relative standard deviation (% 3.1), linear range (33–500 μg L−1), and enrichment factor (52) were calculated. The optimized UIL-DLLME was applied to different water samples. |
| Anahtar Kelimeler |
| Flame atomic absorption spectrometry | Ionic liquid | Microextraction | Microsampler system | Ultrasonication |
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| SCOPUS | 15 |
| Google Scholar | 17 |